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Material World
Process

Alloying and melting

Dissolving one metal into another while molten — the oldest deliberate materials engineering there is, and still how every alloy is made.

An alloy is a solution. Melt a metal, dissolve another element into it, and let it freeze: the second element takes up positions in the first one's crystal lattice, and the resulting metal is not a mixture of two things but a single material with properties neither parent had.

What the addition does is get in the way. A dislocation moving through a pure metal is what lets it deform, and a foreign atom of a different size obstructs that movement. This is why almost every structural metal in use is an alloy, and why the amounts involved are often small — a percent of carbon changes iron more than most people expect of a percent of anything.

Processing

The difficulties are practical rather than conceptual. The elements must be mutually soluble at the temperature used, and stay so on cooling, or the alloy separates into phases as it freezes. Volatile additions boil off — zinc boils below copper's melting point, which is why brass is made by adding zinc to molten copper under conditions that keep it in.

Much modern alloying is done under vacuum or an inert atmosphere, because the reactive elements that improve an alloy most are also the ones that would rather combine with the air.

History

Alloying is the first deliberate materials engineering in the record. Bronze is not a metal anybody found; it is a metal somebody made, by combining two ores or two metals that behave quite differently alone, and getting something harder than either.

That step — the recognition that materials can be designed rather than only discovered — is arguably a larger event than any particular alloy, and it happened long before there was any theory to explain why it worked.

Medium confidence Weak evidence

How we know: checked recently · only one source, so there is nothing to cross-check it against · stated directly by the source.

How this connects

Where a connection has been confirmed by an outside reference, that reference is named beside it.

produces

  • Brass alloy · zinc dissolved into molten copper, under conditions that stop the zinc boiling off
  • Bronze alloy · tin into copper — the first alloy anybody made deliberately
  • Stainless steel alloy · chromium into steel, at the proportion where the oxide film becomes continuous
  • Solder alloy · melted and cast into wire or paste; the alloy is simple and the composition control is not
  • Duralumin alloy · melted and cast, then solution treated and quenched — the strength comes from the heat treatment rather than from the melting
  • Cupronickel alloy · straightforward to make, the two metals being completely soluble in one another at every ratio
  • Pewter alloy · cast in reusable moulds at under 230 °C, which is low enough for a workshop without a serious furnace — much of why it spread
  • Nichrome alloy · melted and drawn to wire, the drawing being the harder half
  • Neodymium magnet alloy · melted, cast, milled to single-crystal powder, pressed in a magnetic field and sintered — the alignment step is what makes it a magnet rather than an alloy
  • Samarium–cobalt magnet alloy · by the same sintering route, and needing no plating afterwards because unlike neodymium it does not corrode
  • Nickel superalloy alloy · vacuum melted, because the reactive elements in it would oxidise in air — and then cast as a single crystal rather than poured
  • 6000 series aluminium alloy alloy · and the composition window is narrow: the magnesium-to-silicon ratio decides whether the precipitate forms usefully
  • Ti-6Al-4V alloy · melted under vacuum or inert gas, because molten titanium reacts with essentially every crucible material and with air
  • Nitinol alloy · melted under vacuum, because oxygen and carbon form inclusions that shift the transformation temperature as well as weakening the alloy
  • 5000 series aluminium alloy alloy · magnesium into aluminium, and it must be melted under cover because magnesium burns
  • 7000 series aluminium alloy alloy · zinc and magnesium into aluminium, then solution treated and aged — the strength comes from the heat treatment, not from the melt
  • Tool steel alloy · carbon and carbide formers into iron, and the carbide is the working part
  • High-speed steel alloy · tungsten, molybdenum, chromium and vanadium into steel, in quantities that keep it hard at the red heat a cutting edge reaches
  • Weathering steel alloy · copper, chromium, nickel and phosphorus at around a per cent between them, which is what makes the rust adherent instead of flaking
  • Invar alloy · thirty-six per cent nickel into iron, at a composition where thermal expansion very nearly cancels
  • Cobalt-chromium alloy alloy · chromium into cobalt, vacuum melted because the alloy is used in bodies and inclusions are failure sites
  • Sterling silver alloy · seven and a half per cent copper into silver, which is the standard because pure silver is too soft to hold a shape
  • Zinc die-casting alloy alloy · aluminium, magnesium and copper into zinc, to a composition tight enough that the name is an acronym of the four ingredients
  • Babbitt metal alloy · tin, antimony and copper, arranged so hard crystals sit in a soft matrix that wears away around them and holds the oil
  • Electrical steel alloy · silicon into iron, and about three per cent is where the rolling mill stops tolerating it
  • Wootz steel alloy · in a sealed crucible, iron and a carbon source held for hours — which is what made it a cast steel a thousand years before anyone else had one
  • Amalgam alloy · the one alloy made without heat: mercury dissolves the other metal at room temperature, which is exactly why it was used in fillings and exactly why it stopped being

takes as input

  • Copper element · the base metal of both brass and bronze
  • Zinc element · the addition that makes brass; it boils below copper's melting point, which is the difficulty
  • Tin element · the addition that hardens copper into bronze
  • Chromium element · the addition that makes steel stainless

succeeded

  • Smelting process · smelting produces the metal; alloying combines metals into something neither was

Sources

  • Material World
    Our own writing

Questions this page answers

Where it comes from, and what it becomes

Follow Alloying and melting back to what it starts as, and forward into what it becomes. Each step is a documented one — a real route material takes, not a chain of inference.

Upstream — what it comes from

  • Alloying and melting → takes as input (the base metal of both brass and bronze) → Copper → is produced by (as blister copper, refined electrolytically afterwards) → Smelting → takes as input (as the element removed, not added) → Oxygen → is produced by (the largest output by tonnage, and the reason air separation units sit beside steelworks) → Air separation → takes as input (the feedstock, and an unusual one in being free, unlimited and available anywhere — the cost is entirely the energy to liquefy it) → Air
  • Alloying and melting → takes as input (the addition that hardens copper into bronze) → Tin → is produced by (reduced from cassiterite at relatively low temperature) → Smelting → takes as input (as the element removed, not added) → Oxygen → is produced by (the largest output by tonnage, and the reason air separation units sit beside steelworks) → Air separation → takes as input (the feedstock, and an unusual one in being free, unlimited and available anywhere — the cost is entirely the energy to liquefy it) → Air
  • Alloying and melting → takes as input (the addition that makes steel stainless) → Chromium → is produced by (as ferrochrome, reduced from chromite and added to steel without ever being separated as the pure metal) → Smelting → takes as input (as the element removed, not added) → Oxygen → is produced by (the largest output by tonnage, and the reason air separation units sit beside steelworks) → Air separation → takes as input (the feedstock, and an unusual one in being free, unlimited and available anywhere — the cost is entirely the energy to liquefy it) → Air
  • Alloying and melting → takes as input (the addition that makes brass; it boils below copper's melting point, which is the difficulty) → Zinc → is produced by (as the oxide, which is then reduced — roasting is the step that makes zinc sulfide smeltable) → Roasting → takes as input (a copper sulfide; roasting drives off the sulfur that would otherwise prevent reduction) → Chalcopyrite
  • Alloying and melting → takes as input (the base metal of both brass and bronze) → Copper → is extracted from (the principal copper ore worldwide) → Chalcopyrite
  • Alloying and melting → takes as input (the addition that hardens copper into bronze) → Tin → is extracted from (the only tin ore of economic importance) → Cassiterite

These are the most distinct paths back. Alloying and melting can be traced through others besides.

Downstream — what it becomes

  • Alloying and melting → produces (melted and cast into wire or paste; the alloy is simple and the composition control is not) → Solder → is used in (every joint on it, and tin-silver-copper since RoHS pushed the lead out from 2006) → Printed circuit board → is used in (and it is the change that made electronics manufacturable: assembly stopped being a wiring job and became a printing one) → Electronics manufacture → is associated with (and the supply chain it produced is the deepest and most concentrated in the world economy) → The semiconductor era complete chain
  • Alloying and melting → produces (chromium into cobalt, vacuum melted because the alloy is used in bodies and inclusions are failure sites) → Cobalt-chromium alloy → is an input to (investment cast, which is how dental frameworks and many implant components are still made) → Casting → produces (investment cast through a spiral selector that admits exactly one crystal orientation, then withdrawn from the furnace over hours so the whole blade grows from it) → Turbine blade → is associated with (the jet engine created the superalloy industry, because no existing material survived the turbine inlet — and turbine temperature has risen about 500 °C since, almost entirely on the blade) → The wartime materials programmes complete chain
  • Alloying and melting → produces (aluminium, magnesium and copper into zinc, to a composition tight enough that the name is an acronym of the four ingredients) → Zinc die-casting alloy → is an input to (hot-chamber die casting at cycle times of seconds, which is the whole economic argument for the alloy) → Casting → produces (investment cast through a spiral selector that admits exactly one crystal orientation, then withdrawn from the furnace over hours so the whole blade grows from it) → Turbine blade → is associated with (the jet engine created the superalloy industry, because no existing material survived the turbine inlet — and turbine temperature has risen about 500 °C since, almost entirely on the blade) → The wartime materials programmes complete chain
  • Alloying and melting → produces (tin, antimony and copper, arranged so hard crystals sit in a soft matrix that wears away around them and holds the oil) → Babbitt metal → is an input to (lined onto a steel or bronze shell, because it has no useful strength of its own) → Casting → produces (investment cast through a spiral selector that admits exactly one crystal orientation, then withdrawn from the furnace over hours so the whole blade grows from it) → Turbine blade → is associated with (the jet engine created the superalloy industry, because no existing material survived the turbine inlet — and turbine temperature has risen about 500 °C since, almost entirely on the blade) → The wartime materials programmes complete chain
  • Alloying and melting → produces (tin into copper — the first alloy anybody made deliberately) → Bronze → is used to make (cast in a two-piece mould with a core, which is what bronze does better than the copper it replaced) → Bronze socketed axe → is associated with → Bronze Age complete chain
  • Alloying and melting → produces (chromium into steel, at the proportion where the oxide film becomes continuous) → Stainless steel → is produced at (discovered here in 1913 by Harry Brearley, investigating gun barrel erosion, and found on a scrap heap because it had not rusted) → Sheffield → is associated with (Bessemer built his first steelworks here in 1858, at the point iron gave way to steel) → Industrial Revolution complete chain

These are the most distinct paths onward. Alloying and melting ends up in others besides.