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Material World
Process · Changes the form, not the material

Heat treatment

Change the properties without changing the composition — the reason two pieces of identical steel can differ by a factor of five in hardness.

Metal is heated and cooled on a controlled schedule to change its internal structure. Nothing is added and nothing is removed: the composition before and after is the same, and the properties can differ by a factor of five.

This is the single most important fact about engineering alloys and the one most often missed. A steel's carbon content sets what it *can* become; the heat treatment sets what it *is*. Quench a medium-carbon steel and it is glass-hard and brittle; temper it and it is a spring; anneal it and it is soft enough to machine — one alloy, three materials.

The mechanisms differ by family. Steel relies on a diffusionless transformation to martensite on rapid cooling; aluminium, nickel and titanium alloys rely on precipitation hardening, where a solution is quenched and then held warm so a fine second phase forms and obstructs dislocation movement. Both are ways of making it harder for the metal to deform internally.

Uses

Hardening and tempering of tools, springs, bearings, gears and cutting edges. Annealing to soften metal between forming operations, and stress relief after welding and machining. Solution treatment and ageing of aluminium, nickel and titanium alloys — the T6 in an aluminium temper designation is exactly this. Case hardening, which gives a gear a hard surface and a tough core by changing only the composition of the outermost skin.

Also normalising to refine the grain of a casting or forging, and the controlled cooling that decides whether a cast iron ends up grey, white or ductile.

History

Empirical for at least three thousand years and understood for barely one. Quench hardening of steel was known across the Iron Age world and passed down as procedure — quench in oil, in urine, in the body of a slave in one particularly persistent classical instruction — with no theory whatsoever behind it.

The explanation arrived with metallography from the 1860s onward and the iron-carbon phase diagram at the turn of the twentieth century. Precipitation hardening in aluminium was discovered accidentally by Alfred Wilm in 1906, who left a quenched alloy over a weekend and found it had hardened by itself; that observation produced Duralumin and, eventually, the all-metal aircraft.

Economic significance

It buys properties with time and energy rather than with alloying elements, which is usually far cheaper — a plain carbon steel correctly heat-treated outperforms an expensively alloyed one that is not.

It is also where a great deal of manufacturing goes wrong: distortion, quench cracking and decarburisation are heat treatment problems, they appear at the end of a part's manufacturing route when all the value has been added, and they scrap finished components rather than raw stock.

Medium confidence Weak evidence

How we know: checked recently · only one source, so there is nothing to cross-check it against · stated directly by the source.

How this connects

Where a connection has been confirmed by an outside reference, that reference is named beside it.

takes as input

  • 6000 series aluminium alloy alloy · solution treated, quenched and aged to T6, which roughly doubles the strength of the annealed material
  • 7000 series aluminium alloy alloy · solution treated and then aged either to peak strength or deliberately past it, trading perhaps a tenth of the strength for resistance to stress corrosion cracking
  • Ti-6Al-4V alloy · annealed, or solution treated and aged where the extra strength is worth the reduced ductility
  • Tool steel alloy · the entire point of the family — supplied soft, machined, then hardened and tempered, because a steel hard enough to cut with cannot itself be cut
  • High-speed steel alloy · hardened from around 1200 °C and tempered two or three times, each temper transforming the austenite the previous one left behind
  • Steel alloy · and the same steel becomes a spring, a cutting edge or a machinable bar depending only on the schedule
  • Nitinol alloy · shape setting is a heat treatment — constrained in the desired geometry at around 500 °C, and that is the shape it remembers
  • Invar alloy · stress relieved and thermally cycled, because residual machining stress relaxes over time and moves the part, which defeats the entire purpose
  • Electrical steel alloy · a box anneal of more than a day above 1,100 °C, during which a few correctly oriented grains grow enormously and consume the rest

is used in

  • Automotive manufacture industry · gears, shafts and springs, and case hardening to give a gear a hard face and a tough core

produces

  • Carbon fibre composite material · laid up as fibre and resin and cured under heat and pressure, usually in an autoclave — and the cure schedule is as much of the specification as the fibre is
  • Glass fibre composite material · the same, and mostly without the autoclave, which is why it costs a fraction as much
  • Plywood material · veneers peeled from a log, laid with the grain of each at right angles to the last, and pressed with adhesive under heat

Sources

  • Wikimedia Foundation · Creative Commons CC0 1.0 Universal (public domain dedication)
  • Material World
    Our own writing

Questions this page answers

Where it comes from, and what it becomes

Follow Heat treatment back to what it starts as, and forward into what it becomes. Each step is a documented one — a real route material takes, not a chain of inference.

Upstream — what it comes from

  • Heat treatment → takes as input (and the same steel becomes a spring, a cutting edge or a machinable bar depending only on the schedule) → Steel → is composed of → Iron → is produced by (as pig iron, high in carbon and brittle until refined) → Smelting → takes as input (as the element removed, not added) → Oxygen → is produced by (the largest output by tonnage, and the reason air separation units sit beside steelworks) → Air separation
  • Heat treatment → takes as input (solution treated, quenched and aged to T6, which roughly doubles the strength of the annealed material) → 6000 series aluminium alloy → is produced by (and the composition window is narrow: the magnesium-to-silicon ratio decides whether the precipitate forms usefully) → Alloying and melting → takes as input (the base metal of both brass and bronze) → Copper → is produced by (as blister copper, refined electrolytically afterwards) → Smelting → takes as input (roasted to drive off sulfur, then reduced to copper) → Chalcopyrite
  • Heat treatment → takes as input (solution treated and then aged either to peak strength or deliberately past it, trading perhaps a tenth of the strength for resistance to stress corrosion cracking) → 7000 series aluminium alloy → is produced by (zinc and magnesium into aluminium, then solution treated and aged — the strength comes from the heat treatment, not from the melt) → Alloying and melting → takes as input (the base metal of both brass and bronze) → Copper → is produced by (as blister copper, refined electrolytically afterwards) → Smelting → takes as input (roasted to drive off sulfur, then reduced to copper) → Chalcopyrite
  • Heat treatment → takes as input (annealed, or solution treated and aged where the extra strength is worth the reduced ductility) → Ti-6Al-4V → is produced by (melted under vacuum or inert gas, because molten titanium reacts with essentially every crucible material and with air) → Alloying and melting → takes as input (the base metal of both brass and bronze) → Copper → is produced by (as blister copper, refined electrolytically afterwards) → Smelting → takes as input (roasted to drive off sulfur, then reduced to copper) → Chalcopyrite
  • Heat treatment → takes as input (the entire point of the family — supplied soft, machined, then hardened and tempered, because a steel hard enough to cut with cannot itself be cut) → Tool steel → is produced by (carbon and carbide formers into iron, and the carbide is the working part) → Alloying and melting → takes as input (the base metal of both brass and bronze) → Copper → is produced by (as blister copper, refined electrolytically afterwards) → Smelting → takes as input (roasted to drive off sulfur, then reduced to copper) → Chalcopyrite
  • Heat treatment → takes as input (hardened from around 1200 °C and tempered two or three times, each temper transforming the austenite the previous one left behind) → High-speed steel → is produced by (tungsten, molybdenum, chromium and vanadium into steel, in quantities that keep it hard at the red heat a cutting edge reaches) → Alloying and melting → takes as input (the base metal of both brass and bronze) → Copper → is produced by (as blister copper, refined electrolytically afterwards) → Smelting → takes as input (roasted to drive off sulfur, then reduced to copper) → Chalcopyrite

These are the most distinct paths back. Heat treatment can be traced through others besides.

Downstream — what it becomes

  • Heat treatment → produces (the same, and mostly without the autoclave, which is why it costs a fraction as much) → Glass fibre composite → is used in (the FR-4 laminate itself: woven glass cloth in flame-retardant epoxy, stiff, dimensionally stable when heated, and self-extinguishing) → Printed circuit board → is used in (and it is the change that made electronics manufacturable: assembly stopped being a wiring job and became a printing one) → Electronics manufacture → is associated with (and the supply chain it produced is the deepest and most concentrated in the world economy) → The semiconductor era complete chain
  • Heat treatment → produces (veneers peeled from a log, laid with the grain of each at right angles to the last, and pressed with adhesive under heat) → Plywood → is associated with (the de Havilland Mosquito was a plywood aeroplane, and it was fast because of it) → The wartime materials programmes complete chain
  • Heat treatment → produces (laid up as fibre and resin and cured under heat and pressure, usually in an autoclave — and the cure schedule is as much of the specification as the fibre is) → Carbon fibre composite → is used as (aircraft primary structure since the 1990s, where stiffness per unit mass is what is being bought) → Structural engineering
  • Heat treatment → is used in (gears, shafts and springs, and case hardening to give a gear a hard face and a tough core) → Automotive manufacture
  • Heat treatment → produces (the same, and mostly without the autoclave, which is why it costs a fraction as much) → Glass fibre composite → is used in (the board everything else is mounted on, which is a thermoset and therefore the part of the phone that most reliably becomes waste) → Smartphone → is used in (and it is where four separate raw-material arguments meet — the 3TG conflict minerals, cobalt, the rare earths, and everything too dispersed to recover) → Electronics manufacture → is associated with (and the supply chain it produced is the deepest and most concentrated in the world economy) → The semiconductor era complete chain
  • Heat treatment → produces (laid up as fibre and resin and cured under heat and pressure, usually in an autoclave — and the cure schedule is as much of the specification as the fibre is) → Carbon fibre composite → is used in (primary structure — a modern wide-body wing and fuselage are more composite than metal) → Aerospace manufacture

These are the most distinct paths onward. Heat treatment ends up in others besides.